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Detection of enantiomers of chiral primary amines by 1H NMR analysis via enamine formation with an enantiopure γ-position aldol product of a β-keto ester
https://oist.repo.nii.ac.jp/records/790
https://oist.repo.nii.ac.jp/records/790fb5872df-9a16-4c6c-a2c0-630c2fd4223d
名前 / ファイル | ライセンス | アクション |
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TL amine resolution 180308 for repository 190118 (237.4 kB)
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Creative Commons Attribution-NonCommercial-NoDerivatives License
(http://creativecommons.org/Licenses/by-nc-nd/4.0/) |
Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2020-05-01 | |||||
タイトル | ||||||
言語 | en | |||||
タイトル | Detection of enantiomers of chiral primary amines by 1H NMR analysis via enamine formation with an enantiopure γ-position aldol product of a β-keto ester | |||||
言語 | ||||||
言語 | eng | |||||
資源タイプ | ||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
資源タイプ | journal article | |||||
著者(英) |
Zhang, Dongxin
× Zhang, Dongxin× Chuang, Po-Shun× Cao, Dong× Krishna, Yarkali× Shilpa, Kola× Tanaka, Fujie |
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書誌情報 |
en : Tetrahedron Letters 巻 59, 号 23, p. 2248-2250, 発行日 2018-04-30 |
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抄録 | ||||||
内容記述タイプ | Other | |||||
内容記述 | A 1H NMR analysis method that detects enantiomers of molecules bearing a primary amino group has been developed. The method uses a β-keto ester-derived probe that forms enamines with the amines and is able to discriminate enantiomers of functionalized amines and amines that have chiral centers at positions remote from the amine group. | |||||
出版者 | ||||||
出版者 | Elsevier | |||||
ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 0040-4039 | |||||
DOI | ||||||
関連タイプ | isVersionOf | |||||
識別子タイプ | DOI | |||||
関連識別子 | info:doi/10.1016/j.tetlet.2018.04.079 | |||||
権利 | ||||||
権利情報 | © 2018 Elsevier Ltd. | |||||
関連サイト | ||||||
識別子タイプ | URI | |||||
関連識別子 | https://www.sciencedirect.com/science/article/pii/S0040403918305653 | |||||
著者版フラグ | ||||||
出版タイプ | AM | |||||
出版タイプResource | http://purl.org/coar/version/c_ab4af688f83e57aa |